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Quantification of Carbohydrates and Related Materials Using Sodium Ion Adducts Produced by Matrix-Assisted Laser Desorption Ionization

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Title
Quantification of Carbohydrates and Related Materials Using Sodium Ion Adducts Produced by Matrix-Assisted Laser Desorption Ionization
Author(s)
Ahn, SH; Park, KM; Moon, JH; Lee, SH; Myung Soo Kim
Subject
Quantification of carbohydrate, ; Quantification of glycan, ; Quantification by MALDI, ; Sodium ion adduct
Publication Date
2016-11
Journal
JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY, v.27, no.11, pp.1887 - 1890
Publisher
SPRINGER
Abstract
The utility of sodium ion adducts produced by matrix-assisted laser desorption ionization for the quantification of analytes with multiple oxygen atoms was evaluated. Uses of homogeneous solid samples and temperature control allowed the acquisition of reproducible spectra. The method resulted in a direct proportionality between the ion abundance ratio I([A + Na](+))/I([M + Na](+)) and the analyte concentration, which could be used as a calibration curve. This was demonstrated for carbohydrates, glycans, and polyether diols with dynamic range exceeding three orders of magnitude. (c) American Society for Mass Spectrometry, 2016
URI
https://pr.ibs.re.kr/handle/8788114/3094
DOI
10.1007/s13361-016-1495-9
ISSN
1044-0305
Appears in Collections:
Center for Nanoparticle Research(나노입자 연구단) > 1. Journal Papers (저널논문)
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