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나노입자 연구단
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Ruthenium-catalyzed redox-neutral and single-step amide synthesis from alcohol and nitrile with complete atom economy

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Title
Ruthenium-catalyzed redox-neutral and single-step amide synthesis from alcohol and nitrile with complete atom economy
Author(s)
Byungjoon Kang; Zhenqian Fu; Soon Hyeok Hong
Publication Date
2013-08
Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, v.135, no.32, pp.11704 - 11707
Publisher
AMER CHEMICAL SOC
Abstract
A completely atom-economical and redoxneutral catalytic amide synthesis from an alcohol and a nitrile is realized. The amide C−N bond is efficiently formed between the nitrogen atom of nitrile and the α- carbon of alcohol, with the help of an N-heterocyclic carbene-based ruthenium catalyst, without a single byproduct. A utility of the reaction was demonstrated by synthesizing 13C or 15N isotope-labeled amides without involvement of any separate reduction and oxidation step.
URI
https://pr.ibs.re.kr/handle/8788114/1271
ISSN
0002-7863
Appears in Collections:
Center for Nanoparticle Research(나노입자 연구단) > Journal Papers (저널논문)
Files in This Item:
21. Ruthenium-Catalyzed Redox-Neutral and Single-Step Amide Synthesis from Alcohol and Nitrile with Complete Atom Economy.pdfDownload

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