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Synthesis of 1,2-amino alcohols via catalytic C–H amidation of sp3 methyl C–H bonds

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Title
Synthesis of 1,2-amino alcohols via catalytic C–H amidation of sp3 methyl C–H bonds
Author(s)
Taek Kang; Heejeong Kim; Jeong Gon Kim; Suk Bok Chang
Publication Date
2014-10
Journal
CHEMICAL COMMUNICATIONS, v.50, no.81, pp.12073 - 12075
Publisher
ROYAL SOC CHEMISTRY
Abstract
Herein a new synthetic route to 1,2-amino alcohols is presented by using C.H amidation of sp3 methyl C.H bonds as a key step. Readily available alcohols were employed as starting materials after converting them to removable ketoxime chelating groups. Iridium catalysts were found to be effective for the C.H amidation, and LAH reduction was then used to furnish b-amino alcohol products.
URI
https://pr.ibs.re.kr/handle/8788114/1461
ISSN
1359-7345
Appears in Collections:
Center for Catalytic Hydrocarbon Functionalizations(분자활성 촉매반응 연구단) > Journal Papers (저널논문)
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